Technology Process of N1-benzyl-N2-phenylbenzene-1,2-diamine
There total 5 articles about N1-benzyl-N2-phenylbenzene-1,2-diamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate;
In
toluene;
at 110 ℃;
for 16.17h;
Inert atmosphere;
DOI:10.1021/ol501766m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C
2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate / toluene / 16.17 h / 110 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium hydride; caesium carbonate;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol501766m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere; Sealed tube
2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate / toluene / 16 h / 110 °C / Sealed tube
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium hydride; caesium carbonate;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1021/acs.joc.5b01872
