4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

Base Information

Chemical Name:4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone
CAS No.:108534-53-8
Molecular Formula:C₂₄H₂₈O₃Si
Molecular Weight:392.57
Hs Code.:

Synonyms:4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

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Chemical Property of 4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

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Technology Process of 4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

There total 6 articles about 4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108534-65-2
tert-Butyl-diphenyl-(1,4,4-trimethoxy-3-methyl-cyclohexa-2,5-dienyloxy)-silane

: 108534-53-8
4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

Guidance literature:: With acetic acid; In water; acetone; for 22h; Ambient temperature;
DOI:10.1021/jo00389a023

Reference yield: 53.0%

: 67-56-1
methanol

: 108534-49-2
tert-butyl-diphenylsilyl 4-hydroxy-3-methylphenyl ether

: 108534-53-8
4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

Guidance literature:: With lutidine; lithium perchlorate; In diethyl ether; at -7 ℃; for 2h; anodic oxidation;
DOI:10.1021/jo00389a023

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 108534-53-8
4-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-2-methyl-cyclohexa-2,5-dienone

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / imidazole / tetrahydrofuran / 1.5 h / Ambient temperature

2: 53 percent / lutidine, LiClO₄ / diethyl ether / 2 h / -7 °C / anodic oxidation

With 1H-imidazole; lutidine; lithium perchlorate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00389a023