(E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

Base Information

Chemical Name:(E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal
CAS No.:488791-30-6
Molecular Formula:C₂₇H₃₃NO₃SSi
Molecular Weight:479.715
Hs Code.:

Synonyms:(E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

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Chemical Property of (E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

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Technology Process of (E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

There total 5 articles about (E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 488791-35-1
4-[(E)-(3S,4S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-hexa-1,5-dienyl]-2-methyl-thiazole

: 488791-30-6
(E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

Guidance literature:: 4-[(E)-(3S,4S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-hexa-1,5-dienyl]-2-methyl-thiazole; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 0 - 25 ℃; for 18h;

With sodium periodate; In methanol; water; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/ja028196l

Reference yield:

: 184246-38-6
(E)-2-methyl-3-(2-methylthiazol-4-yl)acrylaldehyde

: 488791-30-6
(E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

Guidance literature:: Multi-step reaction with 4 steps

1: OsO₄; NMO

2: NaIO₄

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone;
DOI:10.1039/b312213c

Reference yield:

: 470462-89-6
(3S,4S)-4-hydroxy-3,5-dimethyl-6-(2-methylthiazol-4-yl)-1,5-hexadiene

: 488791-30-6
(E)-(2R,3S)-3-(tert-Butoxy-diphenyl-silanyloxy)-2,4-dimethyl-5-(2-methyl-thiazol-4-yl)-pent-4-enal

Guidance literature:: Multi-step reaction with 3 steps

1: OsO₄; NMO

2: NaIO₄

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone;
DOI:10.1039/b312213c