(((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF)

Base Information

• Chemical Name: (((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF)
• CAS No.: 925462-56-2
• Molecular Formula: C₄₁H₆₇N₂OSi₂Y
• Molecular Weight: 749.073
• Mol file: 925462-56-2.mol

Synonyms:(((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF)

Chemical Property of (((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF)

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of (((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF)

There total 2 articles about (((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

[6-(2,4,6-triisopropylphenyl)pyridin-2-yl]-(2,4,6-trimethylphenyl)amine (925461-26-3) + tris(trimethylsilylmethyl)yttrium(bis-tetrahydrofuran) → (((CH3)2CH)3C6H2C5H3NNC6H2(CH3)3)Y(trimethylsilylmethyl)2(THF) (925462-56-2)

Guidance literature:

In hexane; at 0 ℃; Schlenk technique; Glovebox;

DOI:10.1039/c4dt00806e

Reference yield: 62.0%

{[(N-mesityl-6-(2,4,6-triisopropylphenyl)pyridine-2-amine)Y(THF)](μ2-Cl)3Li(THF)2}2 + trimethylsilylmethyllithium (1822-00-0) → (((CH3)2CH)3C6H2C5H3NNC6H2(CH3)3)Y(trimethylsilylmethyl)2(THF) (925462-56-2)

Guidance literature:

In hexane; at 0 - 20 ℃; for 2h; Schlenk technique; Inert atmosphere;

DOI:10.1007/s11172-016-1623-5

Reference yield: 72.0%

1,2-dimethoxyethane (110-71-4) + 2,6-diisopropylbenzenamine (24544-04-5) + (((CH3)2CH)3C6H2C5H3NNC6H2(CH3)3)Y(trimethylsilylmethyl)2(THF) (925462-56-2) → (((CH3)2CH)3C6H2C5H3NNC6H2(CH3)3)Y(trimethylsilylmethyl)(NH-2,6-iPr2C6H3)(DME)

Guidance literature:

2,6-diisopropylbenzenamine; (((CH₃)₂CH)₃C₆H₂C₅H₃NNC₆H₂(CH₃)₃)Y(trimethylsilylmethyl)₂(THF); In hexane; at 20 ℃; for 1h; Schlenk technique;

1,2-dimethoxyethane; Schlenk technique;

DOI:10.1021/om300377h

upstream raw materials:

[6-(2,4,6-triisopropylphenyl)pyridin-2-yl]-(2,4,6-trimethylphenyl)amine

trimethylsilylmethyllithium