(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

Base Information

Chemical Name:(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal
CAS No.:1021942-59-5
Molecular Formula:C₁₈H₁₂Cl₂O₃
Molecular Weight:347.197
Hs Code.:

Synonyms:(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

Suppliers and Price of (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

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Technology Process of (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

There total 1 articles about (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101-84-8
diphenylether

: 1021942-59-5
(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / AlCl₃ / CS₂

2.1: POCl₃ / 0.17 h / 0 °C

2.2: 85 percent / dimethylformamide / 120 h / 4 °C

With aluminium trichloride; trichlorophosphate; In carbon disulfide; 1.1: Friedel-Crafts acylation;
DOI:10.1016/S0040-4020(01)00676-7

Reference yield: 75.0%

: 2365-48-2
Methyl thioglycolate

: 1021942-59-5
(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal

: 250287-35-5
bis[4-(2-methoxycarbonyl-5-thienyl)]phenyl ether

Guidance literature:: Methyl thioglycolate; (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenoxy]-phenyl}-propenal; With triethylamine; In pyridine; at 0 - 50 ℃;

With potassium hydroxide; In pyridine; water; at 10 - 15 ℃; for 0.333333h;
DOI:10.1016/S0040-4020(01)00676-7