2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

Base Information

Chemical Name:2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate
CAS No.:548740-19-8
Molecular Formula:C₂₀H₁₇ClF₆O₅S
Molecular Weight:518.861
Hs Code.:

Synonyms:2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

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Chemical Property of 2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

Chemical Property:

Purity/Quality:

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Technology Process of 2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

There total 3 articles about 2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16484-77-8,18221-59-5,7085-19-0
(R)-Mecoprop

: 450409-87-7
2-[3,5-bis(trifluoromethyl)phenylsulfonyl]-1-ethanol

: 548740-19-8
2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1055/s-2003-36844

Reference yield:

: 130783-02-7
3,5-bis(trifluoromethyl)thiophenol

: 548740-19-8
2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / Et₃N / acetonitrile / 24 h / 20 °C

2: MnSO₄; aq. H₂O₂; NaHCO₃ / acetonitrile / 20 °C

3: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; DMAP / CH₂Cl₂ / 12 h / 20 °C

With dmap; manganese(II) sulfate; dihydrogen peroxide; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1055/s-2003-36844

Reference yield:

: 450409-97-9
2-[3,5-di(trifluoromethyl)phenylsulfanyl]-1-ethanol

: 548740-19-8
2-[3,5-bis(trifluoromethyl)phenylsulfonyl]ethyl 2-(4-chloro-2-methylphenoxy)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: MnSO₄; aq. H₂O₂; NaHCO₃ / acetonitrile / 20 °C

2: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; DMAP / CH₂Cl₂ / 12 h / 20 °C

With dmap; manganese(II) sulfate; dihydrogen peroxide; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetonitrile;
DOI:10.1055/s-2003-36844