benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

Base Information

Chemical Name:benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside
CAS No.:132064-93-8
Molecular Formula:C₁₄H₁₉N₃O₅S
Molecular Weight:341.388
Hs Code.:

Synonyms:benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

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Technology Process of benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

There total 1 articles about benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.9%

: 114413-02-4
benzyl 3-azido-2,3,6-trideoxy-α-L-arabino-hexopyranoside

: 124-63-0
methanesulfonyl chloride

: 132064-93-8
benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

Guidance literature:: With pyridine; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1016/0008-6215(90)80086-I

Reference yield: 81.0%

: 132064-93-8
benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

: 132064-95-0
benzyl 3,4-diazido-2,3,4,6-tetradeoxy-α-L-lyxo-hexopyranoside

Guidance literature:: With sodium azide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 130 ℃; for 16h;
DOI:10.1016/0008-6215(90)80086-I

Reference yield:

: 132064-93-8
benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-arabino-hexopyranoside

: 132064-98-3
benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / sodium azide / hexamethylphosphoric acid triamide / 16 h / 130 °C

2: hydrogen, triethylamine / 10percent Pd-C / ethanol / 8 h / 760 Torr / Ambient temperature

3: 68.36 percent / triethylamine / CH₂Cl₂ / 16 h / 4 °C

With sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane;
DOI:10.1016/0008-6215(90)80086-I