C₃₅H₃₉NO₈

Base Information

Chemical Name:C₃₅H₃₉NO₈
CAS No.:1443752-93-9
Molecular Formula:C₃₅H₃₉NO₈
Molecular Weight:601.697
Hs Code.:

C<sub>35</sub>H<sub>39</sub>NO<sub>8</sub>

Synonyms:C₃₅H₃₉NO₈

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Chemical Property of C₃₅H₃₉NO₈

Chemical Property:

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Technology Process of C₃₅H₃₉NO₈

There total 20 articles about C₃₅H₃₉NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1443752-76-8
(2S)-3-(4-hydroxyphenyl)-4-methyl-2-(4-{2-[(3R)-3-methylpyrrolidin-1-yl]ethoxy}phenyl)-2H-chromen-7-ol

: 541-41-3
chloroformic acid ethyl ester

: 1443752-93-9
C₃₅H₃₉NO₈

Guidance literature:: (2S)-3-(4-hydroxyphenyl)-4-methyl-2-(4-{2-[(3R)-3-methylpyrrolidin-1-yl]ethoxy}phenyl)-2H-chromen-7-ol; With N-ethyl-N,N-diisopropylamine; In ethyl acetate; for 0.0833333h; Cooling with ice;

chloroformic acid ethyl ester; In ethyl acetate; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 108-46-3
recorcinol

: 1443752-93-9
C₃₅H₃₉NO₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: boron trifluoride diethyl etherate / toluene / 1.5 h / 100 - 108 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / 0.75 h / -10 - 0 °C

3.1: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / iso-butanol / 50 - 130 °C / Dean-Stark

4.1: tetrahydrofuran / 1.5 h / 5 - 20 °C

5.1: acetic acid; water / 1.5 h / 90 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

7.1: caesium carbonate; 1,10-Phenanthroline; copper(l) iodide / 91 h / 120 °C / Inert atmosphere

8.1: acetic acid; water / 1 h / 90 °C

9.1: Diacel, Chiralpak IC / hexane; isopropyl alcohol / Resolution of racemate

10.1: N-ethyl-N,N-diisopropylamine / ethyl acetate / 0.08 h / Cooling with ice

10.2: 16 h / 20 °C / Cooling with ice

With piperidine; copper(l) iodide; 1,10-Phenanthroline; boron trifluoride diethyl etherate; water; pyridinium p-toluenesulfonate; caesium carbonate; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; isopropyl alcohol; toluene; iso-butanol;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1443752-93-9
C₃₅H₃₉NO₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: boron trifluoride diethyl etherate / toluene / 1.5 h / 100 - 108 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / 0.75 h / -10 - 0 °C

3.1: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / iso-butanol / 50 - 130 °C / Dean-Stark

4.1: tetrahydrofuran / 1.5 h / 5 - 20 °C

5.1: acetic acid; water / 1.5 h / 90 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

7.1: caesium carbonate; 1,10-Phenanthroline; copper(l) iodide / 91 h / 120 °C / Inert atmosphere

8.1: acetic acid; water / 1 h / 90 °C

9.1: Diacel, Chiralpak IC / hexane; isopropyl alcohol / Resolution of racemate

10.1: N-ethyl-N,N-diisopropylamine / ethyl acetate / 0.08 h / Cooling with ice

10.2: 16 h / 20 °C / Cooling with ice

With piperidine; copper(l) iodide; 1,10-Phenanthroline; boron trifluoride diethyl etherate; water; pyridinium p-toluenesulfonate; caesium carbonate; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; isopropyl alcohol; toluene; iso-butanol;