2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

Base Information

Chemical Name:2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-
CAS No.:154986-10-4
Molecular Formula:C₃₈H₄₀N₅O₁₃P
Molecular Weight:805.735
Hs Code.:

2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-<O,O-diethyl phosphoramidate>

Synonyms:2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

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Chemical Property of 2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

Chemical Property:

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Technology Process of 2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

There total 4 articles about 2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phenoxy-acetic acid (2R,3R,4R,5R)-2-[6-(diethoxy-phosphanylamino)-purin-9-yl]-4-(2-phenoxy-acetoxy)-5-(2-phenoxy-acetoxymethyl)-tetrahydro-furan-3-yl ester

: 154986-10-4
2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

Guidance literature:: With tert.-butylhydroperoxide; In acetonitrile; for 1h; Yield given; Ambient temperature;
DOI:10.1021/ja00101a011

Reference yield:

: 14316-61-1
phenoxyacetic anhydride

: 154986-10-4
2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / 0.17 h / Ambient temperature

2: 1H-tetrazole / acetonitrile / 1 h / Ambient temperature

3: tert-butyl hydroperoxide / acetonitrile / 1 h / Ambient temperature

With pyridine; 1H-tetrazole; tert.-butylhydroperoxide; In acetonitrile;
DOI:10.1021/ja00101a011

Reference yield:

: 154971-68-3
2',3',5'-tris-O-(phenoxyacetyl)adenosine

: 154986-10-4
2',3',5'-tri-O-(phenoxyacetyl)adenosine 6-N-

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / acetonitrile / 1 h / Ambient temperature

2: tert-butyl hydroperoxide / acetonitrile / 1 h / Ambient temperature

With 1H-tetrazole; tert.-butylhydroperoxide; In acetonitrile;
DOI:10.1021/ja00101a011