C₃₂H₂₆Cl₃NO₁₀

Base Information

Chemical Name:C₃₂H₂₆Cl₃NO₁₀
CAS No.:1122631-50-8
Molecular Formula:C₃₂H₂₆Cl₃NO₁₀
Molecular Weight:690.918
Hs Code.:

C<sub>32</sub>H<sub>26</sub>Cl<sub>3</sub>NO<sub>10</sub>

Synonyms:C₃₂H₂₆Cl₃NO₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₂₆Cl₃NO₁₀

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Technology Process of C₃₂H₂₆Cl₃NO₁₀

There total 9 articles about C₃₂H₂₆Cl₃NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: C₃₀H₂₆O₁₀

: 545-06-2
trichloroacetonitrile

: 1122631-50-8
C₃₂H₂₆Cl₃NO₁₀

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol802915h

Reference yield:

: 54325-28-9
6-O-trityl-D-glucopyranose

: 1122631-50-8
C₃₂H₂₆Cl₃NO₁₀

: C₃₂H₂₆Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 16 h / 0 °C

2: sulfuric acid; water / dichloromethane / 1 h

3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite

4: potassium carbonate; 18-crown-6 ether / tetrahydrofuran / 2 h

5: hydrogen bromide; acetic acid / dichloromethane

6: water; silver carbonate / acetone

7: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane

With pyridine; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 18-crown-6 ether; sulfuric acid; water; hydrogen bromide; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; silver carbonate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.3390/molecules180911198

Reference yield:

: 247017-29-4
1,2,3,4-tetra-O-benzoyl-6-O-trityl-α,β-D-glucopyranoside

: 1122631-50-8
C₃₂H₂₆Cl₃NO₁₀

: C₃₂H₂₆Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid; water / dichloromethane / 1 h

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite

3: potassium carbonate; 18-crown-6 ether / tetrahydrofuran / 2 h

4: hydrogen bromide; acetic acid / dichloromethane

5: water; silver carbonate / acetone

6: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 18-crown-6 ether; sulfuric acid; water; hydrogen bromide; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; silver carbonate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.3390/molecules180911198