(R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1238945-31-7
Molecular Formula:C₁₆H₂₉BO₂
Molecular Weight:264.216
Hs Code.:

Synonyms:(R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about (R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 155184-90-0
(E)-3-cyclohexylbut-2-en-1-yl methyl carbonate

: 73183-34-3
bis(pinacol)diborane

: 1238945-31-7
(R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (C₆H₅)2C₃N₂H₃((CH₃)3C₆H₂)C₆H₄SO₃; sodium methylate; copper(II) bis(trifluoromethanesulfonate); In 1,2-dimethoxyethane; at -30 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja104254d

Reference yield:

: 1238945-31-7
(R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 98837-46-8
N-benzylidenediphenylphosphinamide

: 1424357-79-8
N-((1S,2R)-2-cyclohexyl-2-methyl-1-phenylbut-3-en-1-yl)-P,P-diphenylphosphinic amide

: N-(2-cyclohexyl-2-methyl-1-phenylbut-3-en-1-yl)-P,P-diphenylphosphinic amide

Guidance literature:: With methanol; (S)-N-(3-(tert-butyl)-2-hydroxybenzyl)-1-(dimethylamino)-3-methyl-1-oxobutan-2-aminium; bis(t-butoxy) zinc; In toluene; at 50 ℃; for 18h; Overall yield = 70 %; Inert atmosphere;

Reference yield:

: 1238945-31-7
(R)-2-(2-cyclohexylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 98837-46-8,67764-52-7
P,P-diphenyl-N-(phenylmethylene)phosphinic amide

: 1424357-79-8
N-((1S,2R)-2-cyclohexyl-2-methyl-1-phenylbut-3-en-1-yl)-P,P-diphenylphosphinic amide

: N-(2-cyclohexyl-2-methyl-1-phenylbut-3-en-1-yl)-P,P-diphenylphosphinic amide

Guidance literature:: With (S)-N-(3-(tert-butyl)-2-hydroxybenzyl)-1-(dimethylamino)-3-methyl-1-oxobutan-2-aminium; sodium t-butanolate; In methanol; toluene; at 22 ℃; for 18h; Overall yield = 70 %; enantioselective reaction; Inert atmosphere;
DOI:10.1038/nature11844