C₄₉H₆₃N₅O₈

Base Information

Chemical Name:C₄₉H₆₃N₅O₈
CAS No.:1262241-19-9
Molecular Formula:C₄₉H₆₃N₅O₈
Molecular Weight:850.068
Hs Code.:

C<sub>49</sub>H<sub>63</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:C₄₉H₆₃N₅O₈

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Chemical Property of C₄₉H₆₃N₅O₈

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Technology Process of C₄₉H₆₃N₅O₈

There total 8 articles about C₄₉H₆₃N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1262241-18-8
Fmoc-Pro-Ile-Val-Phe-OH

: 247068-85-5
(S)-2-amino-4-methyl-1-((R)-2-methyloxiran-2-yl)pentan-1-one trifluoroacetic acid salt

: 1262241-19-9
C₄₉H₆₃N₅O₈

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 4 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/ja109377p

Reference yield:

: C₁₇H₂₅NO₃

: 1262241-19-9
C₄₉H₆₃N₅O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / decane; dichloromethane / 18 h / 4 - 20 °C / Inert atmosphere

1.2: 27 h / 4 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / 1.33 h / 20 °C / 760.05 Torr / Inert atmosphere

3.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3.5 h / 4 - 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In decane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja109377p

Reference yield:

: 869487-76-3
(S)-benzyl (2,6-dimethyl-3-oxohept-1-en-4-yl)carbamate

: 1262241-19-9
C₄₉H₆₃N₅O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 3 h / 0 °C / Inert atmosphere

2.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / decane; dichloromethane / 18 h / 4 - 20 °C / Inert atmosphere

2.2: 27 h / 4 - 20 °C

3.1: palladium 10% on activated carbon; hydrogen / 1.33 h / 20 °C / 760.05 Torr / Inert atmosphere

4.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3.5 h / 4 - 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; sodium tetrahydroborate; bis(acetylacetonate)oxovanadium; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; decane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja109377p