3'-methoxy-E-diethylstilbestrol dibenzoate

Base Information

Chemical Name:3'-methoxy-E-diethylstilbestrol dibenzoate
CAS No.:1369506-06-8
Molecular Formula:C₃₃H₃₀O₅
Molecular Weight:506.598
Hs Code.:

Synonyms:3'-methoxy-E-diethylstilbestrol dibenzoate

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Chemical Property of 3'-methoxy-E-diethylstilbestrol dibenzoate

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Technology Process of 3'-methoxy-E-diethylstilbestrol dibenzoate

There total 5 articles about 3'-methoxy-E-diethylstilbestrol dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 908108-37-2
3-(4-hydroxy-3-methoxyphenyl)-4-(4-hydroxyphenyl)hex-3-ene

: 98-88-4
benzoyl chloride

: 1369506-06-8
3'-methoxy-E-diethylstilbestrol dibenzoate

Guidance literature:: With potassium carbonate; In dichloromethane; for 3h; Reflux;
DOI:10.1016/j.steroids.2011.12.024

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1369506-06-8
3'-methoxy-E-diethylstilbestrol dibenzoate

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trifluoride diethyl etherate / 19 h / 65 °C

2.1: potassium carbonate / acetone / 10 h / Reflux

3.1: sodium hydride / toluene / 0.5 h / Reflux

3.2: 16 h / 25 °C / Reflux

4.1: tetrahydrofuran / 3 h / 35 °C / Inert atmosphere

5.1: sulfuric acid / acetone / 0.5 h / 20 °C

6.1: 5%-palladium/activated carbon; ammonium formate / methanol; dichloromethane / 1 h / 20 °C

7.1: hydrogen bromide; acetic acid / 48 h / 20 °C

8.1: potassium carbonate / dichloromethane / 3 h / Reflux

With sulfuric acid; 5%-palladium/activated carbon; boron trifluoride diethyl etherate; hydrogen bromide; ammonium formate; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 4.1: Grignard reaction;
DOI:10.1016/j.steroids.2011.12.024

Reference yield:

: 1202248-59-6
1-(4-hydroxy-3-methoxyphenyl)-2-(4-hydroxyphenyl)ethanone

: 1369506-06-8
3'-methoxy-E-diethylstilbestrol dibenzoate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetone / 10 h / Reflux

2.1: sodium hydride / toluene / 0.5 h / Reflux

2.2: 16 h / 25 °C / Reflux

3.1: tetrahydrofuran / 3 h / 35 °C / Inert atmosphere

4.1: sulfuric acid / acetone / 0.5 h / 20 °C

5.1: 5%-palladium/activated carbon; ammonium formate / methanol; dichloromethane / 1 h / 20 °C

6.1: hydrogen bromide; acetic acid / 48 h / 20 °C

7.1: potassium carbonate / dichloromethane / 3 h / Reflux

With sulfuric acid; 5%-palladium/activated carbon; hydrogen bromide; ammonium formate; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 3.1: Grignard reaction;
DOI:10.1016/j.steroids.2011.12.024