1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

Base Information

Chemical Name:1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone
CAS No.:791124-58-8
Molecular Formula:C₃₇H₄₆O₆S
Molecular Weight:618.835
Hs Code.:

Synonyms:1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

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Chemical Property of 1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

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Technology Process of 1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

There total 4 articles about 1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 791124-56-6
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

: 791124-58-8
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

Guidance literature:: With sodium periodate; In water; acetonitrile; at 70 ℃; for 48h;
DOI:10.1016/j.bmc.2004.08.014

Reference yield:

: 109121-38-2
2,5-anhydro-3,4,6-tri-O-benzyl-1-deoxy-1-iodo-D-glucitol

: 791124-58-8
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / dimethylformamide / 12 h / 20 °C

2: 97 percent / lithium aluminum hydride / diethyl ether / 1 h / 20 °C

3: 76 percent / n-butyl lithium / tetrahydrofuran / 2 h / -78 - 20 °C

4: 53 percent / sodium periodate / acetonitrile; H₂O / 48 h / 70 °C

With sodium periodate; lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2004.08.014

Reference yield:

: 33169-56-1
(2E,6E)-3,7-dimethyl-1-p-tolylsulfonyl-2,6-octadiene

: 791124-58-8
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / n-butyl lithium / tetrahydrofuran / 2 h / -78 - 20 °C

2: 53 percent / sodium periodate / acetonitrile; H₂O / 48 h / 70 °C

With sodium periodate; n-butyllithium; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/j.bmc.2004.08.014