3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

Base Information

Chemical Name:3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate
CAS No.:791124-37-3
Molecular Formula:C₂₉H₃₂O₅S
Molecular Weight:492.636
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

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Chemical Property of 3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

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Technology Process of 3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

There total 1 articles about 3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 109121-38-2
2,5-anhydro-3,4,6-tri-O-benzyl-1-deoxy-1-iodo-D-glucitol

: 10387-40-3
potassium thioacetate

: 791124-37-3
3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2004.08.014

Reference yield: 97.0%

: 791124-37-3
3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

: 791124-48-6
3,4,6-tri-O-benzyl-2,5-anhydroglucityl thiol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2004.08.014

Reference yield:

: 791124-37-3
3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

: 791124-58-8
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / lithium aluminum hydride / diethyl ether / 1 h / 20 °C

2: 76 percent / n-butyl lithium / tetrahydrofuran / 2 h / -78 - 20 °C

3: 53 percent / sodium periodate / acetonitrile; H₂O / 48 h / 70 °C

With sodium periodate; lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether; water; acetonitrile;
DOI:10.1016/j.bmc.2004.08.014