1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

Base Information

Chemical Name:1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide
CAS No.:791124-56-6
Molecular Formula:C₃₇H₄₆O₄S
Molecular Weight:586.836
Hs Code.:

Synonyms:1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

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Chemical Property of 1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

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Technology Process of 1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

There total 3 articles about 1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 33169-56-1
(2E,6E)-3,7-dimethyl-1-p-tolylsulfonyl-2,6-octadiene

: 791124-48-6
3,4,6-tri-O-benzyl-2,5-anhydroglucityl thiol

: 791124-56-6
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃; for 2h;
DOI:10.1016/j.bmc.2004.08.014

Reference yield:

: 109121-38-2
2,5-anhydro-3,4,6-tri-O-benzyl-1-deoxy-1-iodo-D-glucitol

: 791124-56-6
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / dimethylformamide / 12 h / 20 °C

2: 97 percent / lithium aluminum hydride / diethyl ether / 1 h / 20 °C

3: 76 percent / n-butyl lithium / tetrahydrofuran / 2 h / -78 - 20 °C

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.08.014

Reference yield:

: 791124-37-3
3,4,6-tri-O-benzyl-2,5-anhydroglucityl thioacetate

: 791124-56-6
1-geranyl 3,4,6-tri-O-benzyl-2,5-anhydroglucityl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / lithium aluminum hydride / diethyl ether / 1 h / 20 °C

2: 76 percent / n-butyl lithium / tetrahydrofuran / 2 h / -78 - 20 °C

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmc.2004.08.014