methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

Base Information

Chemical Name:methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate
CAS No.:204571-89-1
Molecular Formula:C₂₉H₂₆O₄
Molecular Weight:438.523
Hs Code.:

Synonyms:methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

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Chemical Property of methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

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Technology Process of methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

There total 7 articles about methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98288-51-8
2-(3-bromophenyl)acetyl chloride

: 204571-89-1
methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

Guidance literature:: Multi-step reaction with 6 steps

1: AlCl₃ / 1,2-dichloro-ethane / 15 h / 50 °C

2: 77 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2N aq. Na₂CO₃ / toluene / 14 h / Heating

3: 2N aq. KOH / dimethylsulfoxide / 1 h / 60 °C

4: 1.) hydrazine hydrate, 2.) t-BuOK / 1.) 60 deg C, 1 h, 2.) 100 deg C, 18 h

5: BBr₃ / CH₂Cl₂ / 4 h / -78 - 0 °C

6: H₂SO₄ / Heating

With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; aluminium trichloride; sulfuric acid; potassium tert-butylate; boron tribromide; sodium carbonate; hydrazine hydrate; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jm9704917

Reference yield:

: 171905-89-8
methyl 3-(2-methoxyphenyl)phenylacetate

: 204571-89-1
methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

Guidance literature:: Multi-step reaction with 6 steps

1: AlCl₃ / 1,2-dichloro-ethane / 15 h / 50 °C

2: 77 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2N aq. Na₂CO₃ / toluene / 14 h / Heating

3: 2N aq. KOH / dimethylsulfoxide / 1 h / 60 °C

4: 1.) hydrazine hydrate, 2.) t-BuOK / 1.) 60 deg C, 1 h, 2.) 100 deg C, 18 h

5: BBr₃ / CH₂Cl₂ / 4 h / -78 - 0 °C

6: H₂SO₄ / Heating

With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; aluminium trichloride; sulfuric acid; potassium tert-butylate; boron tribromide; sodium carbonate; hydrazine hydrate; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jm9704917

Reference yield:

: 204571-87-9
methyl 3-{2-methoxy-5-[1-oxo-2-(3-bromophenyl)ethyl]phenyl}phenylacetate

: 204571-89-1
methyl 3-(2-hydroxy-5-{2-[3-(2-hydroxyphenyl)phenyl]ethyl}phenyl)phenylacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2N aq. Na₂CO₃ / toluene / 14 h / Heating

2: 2N aq. KOH / dimethylsulfoxide / 1 h / 60 °C

3: 1.) hydrazine hydrate, 2.) t-BuOK / 1.) 60 deg C, 1 h, 2.) 100 deg C, 18 h

4: BBr₃ / CH₂Cl₂ / 4 h / -78 - 0 °C

5: H₂SO₄ / Heating

With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium tert-butylate; boron tribromide; sodium carbonate; hydrazine hydrate; In dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jm9704917