2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Base Information

Chemical Name:2-methyl-1-benzyl>-1-pyrrolinium perchlorate
CAS No.:92014-49-8
Molecular Formula:C₁₆H₂₆NSi*ClO₄
Molecular Weight:359.925
Hs Code.:

2-methyl-1-<o-<(trimethylsilyl)methyl>benzyl>-1-pyrrolinium perchlorate

Synonyms:2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Suppliers and Price of 2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-methyl-1-benzyl>-1-pyrrolinium perchlorate

There total 5 articles about 2-methyl-1-benzyl>-1-pyrrolinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 872-32-2
2-methyl-1H-pyrroline

: 104330-78-1
2-(trimethylsilylmethyl)benzyl bromide

: 92014-49-8
2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Guidance literature:: With silver perchlorate; In acetonitrile; for 1h;
DOI:10.1021/ja00243a029

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 92014-49-8
2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Guidance literature:: Multi-step reaction with 4 steps

1: n-BuLi, tetramethylethylenediamine / tetrahydrofuran / 3.5 h / 25 °C

2: 87 percent / H₂SO₄ / tetrahydrofuran; H₂O / 2 h

3: 97 percent / triphenylphosphine, CBr₄ / diethyl ether / 0.5 h / 25 °C

4: 41 percent / AgClO₄ / acetonitrile / 1 h

With n-butyllithium; carbon tetrabromide; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; silver perchlorate; triphenylphosphine; In tetrahydrofuran; diethyl ether; water; acetonitrile;
DOI:10.1021/ja00243a029

Reference yield:

: 57754-01-5
2-[(trimethylsilyl)methyl]benzyl alcohol

: 92014-49-8
2-methyl-1-benzyl>-1-pyrrolinium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / triphenylphosphine, CBr₄ / diethyl ether / 0.5 h / 25 °C

2: 41 percent / AgClO₄ / acetonitrile / 1 h

With carbon tetrabromide; silver perchlorate; triphenylphosphine; In diethyl ether; acetonitrile;
DOI:10.1021/ja00243a029