Diazald(R)-N-methyl-d3

Base Information

Chemical Name:Diazald(R)-N-methyl-d3
CAS No.:42366-72-3
Molecular Formula:C₈H₁₀N₂O₃S
Molecular Weight:217.221
Hs Code.:
European Community (EC) Number:610-021-2
DSSTox Substance ID:DTXSID101230663
Mol file:42366-72-3.mol

Synonyms:42366-72-3;Diazald(R)-N-methyl-d3;4-methyl-N-nitroso-N-(trideuteriomethyl)benzenesulfonamide;N-Methyl-N-nitrosotoluene-4-sulfonamide-d3;Diazald-d3;HY-Y0544S;DTXSID101230663;DIAZALD(R)-(N-METHYL-D3);AKOS015916076;CS-0567880;D99179;4-Methyl-N-(methyl-d3)-N-nitrosobenzenesulfonamide;Diazald(R)-(N-methyl-d3), 98 atom % D, 97% (CP)

Suppliers and Price of Diazald(R)-N-methyl-d3

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-METHYL-D3-N-NITROSO-PARA-TOLUENESULFONAMIDE 95.00%
5MG
$ 501.15

Total 24 raw suppliers

Chemical Property of Diazald(R)-N-methyl-d3

Chemical Property:

Melting Point:60-63oC
PSA：75.19000
LogP:2.37770
Storage Temp.:0-6°C
XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:217.06004360
Heavy Atom Count:14
Complexity:288

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-METHYL-D3-N-NITROSO-PARA-TOLUENESULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn,Xi,E
Statements: 20/21/22-43-36/37/38-2
Safety Statements: 26-36-36/37-35-15

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N(C)N=O
Isomeric SMILES:[2H]C([2H])([2H])N(N=O)S(=O)(=O)C1=CC=C(C=C1)C

Technology Process of Diazald(R)-N-methyl-d3

There total 6 articles about Diazald(R)-N-methyl-d3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85894-45-7
4-methyl-N-(methyl-d₃)benzenesulfonamide

: 42366-72-3
N-methyl-d₃-N-nitroso-para-toluenesulfonamide

Guidance literature:: With sodium acetate; acetic acid; sodium chloride; sodium nitrite; In water; at 0 ℃;
DOI:10.1002/jlcr.3231

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 42366-72-3
N-methyl-d₃-N-nitroso-para-toluenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; dmap / dichloromethane / 2.42 h / 23 °C

2: potassium carbonate / acetonitrile / 18 h / 80 °C

3: trifluoroacetic acid / neat (no solvent) / 1 h / 0 - 20 °C

4: sodium chloride; sodium acetate; sodium nitrite; acetic acid / water / 0 °C

With dmap; sodium acetate; potassium carbonate; acetic acid; triethylamine; trifluoroacetic acid; sodium chloride; sodium nitrite; In dichloromethane; water; acetonitrile;
DOI:10.1002/jlcr.3231

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 42366-72-3
N-methyl-d₃-N-nitroso-para-toluenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 18 h / 80 °C

2: trifluoroacetic acid / neat (no solvent) / 1 h / 0 - 20 °C

3: sodium chloride; sodium acetate; sodium nitrite; acetic acid / water / 0 °C

With sodium acetate; potassium carbonate; acetic acid; trifluoroacetic acid; sodium chloride; sodium nitrite; In water; acetonitrile;
DOI:10.1002/jlcr.3231