cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

Base Information

Chemical Name:cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside
CAS No.:160204-46-6
Molecular Formula:C₃₂H₅₀O₆Si₂
Molecular Weight:586.916
Hs Code.:

Synonyms:cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

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Chemical Property of cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

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Technology Process of cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

There total 4 articles about cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 160204-41-1
cyclohexyl 2,3-di-O-benzyl-β-D-mannopyranoside

: 160204-46-6
cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)89567-3

Reference yield:

: 68536-42-5
acetyl 4,6-di-O-acetate-2,3-di-O-benzyl-α-D-mannopyranoside

: 160204-46-6
cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen bromide / CH₂Cl₂; acetic acid / 0 °C

2: silver silicate / toluene / 0.5 h / -15 °C

3: 87 percent / triethylamine / methanol; H₂O

4: 86 percent / trifluoroacetic acid / CH₂Cl₂

With silver silicate; hydrogen bromide; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; water; acetic acid; toluene;
DOI:10.1016/S0040-4020(01)89567-3

Reference yield:

: 95504-11-3
1,4-di-O-acetyl-2,3-di-O-benzyl-α-D-mannopyranosyl bromide

: 160204-46-6
cyclohexyl 2,3-di-O-benzyl-4,6-bis-O-trimethylsilyl-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: silver silicate / toluene / 0.5 h / -15 °C

2: 87 percent / triethylamine / methanol; H₂O

3: 86 percent / trifluoroacetic acid / CH₂Cl₂

With silver silicate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; water; toluene;
DOI:10.1016/S0040-4020(01)89567-3