4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid

Base Information

• Chemical Name: 4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid
• CAS No.: 79839-41-1
• Molecular Formula: C₂₀H₂Cl₁₄O₂
• Molecular Weight: 770.577
• Mol file: 79839-41-1.mol

Synonyms:4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid

Chemical Property of 4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid

There total 1 articles about 4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.9%

αH-(Heptadecachloro-4-methyltriphenyl)methane (78227-02-8) → 4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid (79839-41-1)

Guidance literature:

With sulfuric acid; at 110 - 120 ℃; for 90h;

DOI:10.1021/jo00341a015

Reference yield: 96.7%

4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid (79839-41-1) → ammonium α-H-tetradecachlorotriphenylmethane-4-carboxylate (79839-42-2)

Guidance literature:

With ammonia; In diethyl ether; for 0.5h;

DOI:10.1021/jo00341a015

Reference yield: 89.0%

tetra(n-butyl)ammonium hydroxide (2052-49-5) + 4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorobenzoic acid (79839-41-1) → Tetra-n-butylammonium 4-carboxylatotetradecachlorotriphenylmethide (126061-88-9)

Guidance literature:

In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jo00297a017

upstream raw materials:

αH-(Heptadecachloro-4-methyltriphenyl)methane

Downstream raw materials:

Methyl αH-(tetradecachlorotriphenyl)methane-4-carboxylate

Tetra-n-butylammonium 4-carboxylatotetradecachlorotriphenylmethide

4-Carboxylatotetradecachlorotriphenylmethyl Radical

4-iodotetradecachlorotriphenylmethyl radical