(E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:(E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate
CAS No.:1396629-91-6
Molecular Formula:C₂₂H₁₇F₃N₂O₅S
Molecular Weight:478.449
Hs Code.:

Synonyms:(E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

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Chemical Property of (E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of (E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

There total 4 articles about (E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1334682-12-0
trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

: 104-94-9
4-methoxy-aniline

: 1396629-91-6
(E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

Guidance literature:: With sodium hydrogencarbonate; In toluene; at 100 ℃; Molecular sieve; Inert atmosphere; Sealed tube;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j

Reference yield:

: 1334683-40-7
C₁₄H₁₁NO₃

: 1396629-91-6
(E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / toluene / 100 °C / Molecular sieve; Inert atmosphere; Sealed tube

With pyridine; sodium hydrogencarbonate; In dichloromethane; toluene;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j

Reference yield:

: 611-73-4
Benzoylformic acid

: 1396629-91-6
(E)-2-(2-((4-methoxyphenyl)imino)-2-phenylacetamido)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4: sodium hydrogencarbonate / toluene / 100 °C / Molecular sieve; Inert atmosphere; Sealed tube

With pyridine; oxalyl dichloride; sodium hydrogencarbonate; triethylamine; N,N-dimethyl-formamide; In dichloromethane; toluene;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j