S-phenyl 4-phenylbutanethioate

Base Information

• Chemical Name: S-phenyl 4-phenylbutanethioate
• CAS No.: 75056-46-1
• Molecular Formula: C₁₆H₁₆OS
• Molecular Weight: 256.368
• Mol file: 75056-46-1.mol

Synonyms:S-phenyl 4-phenylbutanethioate

Chemical Property of S-phenyl 4-phenylbutanethioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-phenyl 4-phenylbutanethioate

There total 3 articles about S-phenyl 4-phenylbutanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

carbon monoxide (201230-82-2) + 1-Bromo-3-phenylpropane (637-59-2) + thiophenol (108-98-5) → S-phenyl 4-phenylbutanethioate (75056-46-1)

Guidance literature:

With di-μ-chlorobis(norbornadiene)dirhodium(I); 1,3-bis-(diphenylphosphino)propane; sodium fluoride; sodium iodide; In 1,4-dioxane; at 140 ℃; for 12h; under 4500.45 Torr; Sealed tube;

DOI:10.1039/d0cc07578g

Reference yield: 55.0%

4-phenyl-1,1,1-tris(phenylthio)butane (111171-84-7) → S-phenyl 4-phenylbutanethioate (75056-46-1) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0)

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

thiophenol (108-98-5) + 4-Phenylbutyric acid (1821-12-1) → S-phenyl 4-phenylbutanethioate (75056-46-1)

Guidance literature:

With 2-fluoro-1-ethylpyridinium tetrafluoroborate; cesium fluoride; Yield given. Multistep reaction; 1) methylene chloride, 30 min, r.t., 2) methylene chloride, 3 h, r.t.;

DOI:10.1246/cl.1980.391

upstream raw materials:

4-phenyl-1,1,1-tris(phenylthio)butane

thiophenol

4-Phenylbutyric acid

carbon monoxide

Downstream raw materials:

allylbenzene

1-propenylbenzene

cis-1-phenyl-1-propylene