Technology Process of C32H35N3O5
There total 5 articles about C32H35N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H25NO3; phenyl isocyanate;
With
bis(p-methoxyphenyl)methanone;
In
acetonitrile;
at 20 ℃;
for 8.5h;
UV-irradiation;
methanol;
In
acetonitrile;
for 16h;
DOI:10.1021/ol200772f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 4-methyl-morpholine; osmium(VIII) oxide; water / tetrahydrofuran / 4.5 h / 20 °C
2.1: pyridinium p-toluenesulfonate / dichloromethane / 0.83 h / Reflux
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux
4.1: bis(p-methoxyphenyl)methanone / acetonitrile / 8.5 h / 20 °C / UV-irradiation
4.2: 16 h
With
4-methyl-morpholine; osmium(VIII) oxide; lithium aluminium tetrahydride; bis(p-methoxyphenyl)methanone; water; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol200772f
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / toluene / 11 h / 140 °C
2.1: 4-methyl-morpholine; osmium(VIII) oxide; water / tetrahydrofuran / 4.5 h / 20 °C
3.1: pyridinium p-toluenesulfonate / dichloromethane / 0.83 h / Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux
5.1: bis(p-methoxyphenyl)methanone / acetonitrile / 8.5 h / 20 °C / UV-irradiation
5.2: 16 h
With
4-methyl-morpholine; osmium(VIII) oxide; lithium aluminium tetrahydride; bis(p-methoxyphenyl)methanone; water; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ol200772f
