(-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

Base Information

Chemical Name:(-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside
CAS No.:120041-98-7
Molecular Formula:C₁₉H₂₉NO₈
Molecular Weight:399.441
Hs Code.:

Synonyms:(-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

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Chemical Property of (-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

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Technology Process of (-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

There total 9 articles about (-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 120041-97-6
(-)-benzyl 3-deoxy-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

: 107-30-2
chloromethyl methyl ether

: 120041-98-7
(-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 0.5h; Heating;
DOI:10.1016/S0040-4020(01)81431-9

Reference yield:

: 97989-81-6
(-)-benzyl β-D-gentosaminide

: 120041-98-7
(-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / anhydrous K₂CO₃ / acetone / 1 h / Heating

2: 97 percent / ethyldiisopropylamine / tetrahydrofuran / 0.5 h / Heating

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)81431-9

Reference yield:

: 67412-71-9
(-)-benzyl 2,3-anhydro-β-D-ribopyranoside

: 120041-98-7
(-)-benzyl 3-deoxy-2,4-bis-(O-methoxymethyl)-3-(N-methoxycarbonyl-N-methylamino)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / methanol / 24 h / 60 °C

2: 85 percent / anhydrous K₂CO₃ / acetone / 1 h / Heating

3: 97 percent / ethyldiisopropylamine / tetrahydrofuran / 0.5 h / Heating

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; acetone;
DOI:10.1016/S0040-4020(01)81431-9