Benzyl 2-o-(methylsulfonyl)pentopyranoside

Base Information

Chemical Name:Benzyl 2-o-(methylsulfonyl)pentopyranoside
CAS No.:7143-64-8
Molecular Formula:C13H18O7S
Molecular Weight:318.3428
Hs Code.:
NSC Number:39268
DSSTox Substance ID:DTXSID20284840

Synonyms:7143-64-8;benzyl 2-o-(methylsulfonyl)pentopyranoside;NSC39268;DTXSID20284840;NSC-39268;A843992;[4,5-bis(oxidanyl)-2-phenylmethoxy-oxan-3-yl] methanesulfonate;methanesulfonic acid (4,5-dihydroxy-2-phenylmethoxy-3-oxanyl) ester

Suppliers and Price of Benzyl 2-o-(methylsulfonyl)pentopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Benzyl 2-o-(methylsulfonyl)pentopyranoside

Chemical Property:

Vapor Pressure:8.64E-13mmHg at 25°C
Boiling Point:546.8°Cat760mmHg
Flash Point:284.5°C
Density:1.43g/cm³
XLogP3:-0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:318.07732408
Heavy Atom Count:21
Complexity:413

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)OC1C(C(COC1OCC2=CC=CC=C2)O)O

Technology Process of Benzyl 2-o-(methylsulfonyl)pentopyranoside

There total 6 articles about Benzyl 2-o-(methylsulfonyl)pentopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 6336-16-9
benzyl 3,4-O-isopropylidene-β-D-arabinopyranoside

: 7143-64-8
(-)-benzyl 2-O-methanesulfonyl-β-D-arabinopyranoside

Guidance literature:: With pyridine; Erhitzen des Reaktionsprodukts mit wss. Schwefelsaeure und Aceton;
DOI:10.1021/ja01552a056

Reference yield:

: 120041-96-5
benzyl 3,4-O-isopropylidene-2-O-methanesulfonyl-β-D-arabinopyranoside

: 7143-64-8
(-)-benzyl 2-O-methanesulfonyl-β-D-arabinopyranoside

Guidance literature:: With sulfuric acid; In acetone; for 0.0833333h; Yield given; Heating;
DOI:10.1016/S0040-4020(01)81431-9

Reference yield:

: 87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2
(-)-D-arabinose

: 7143-64-8
(-)-benzyl 2-O-methanesulfonyl-β-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / HCl / 18 h / Ambient temperature

2: 95 percent / p-toluenesulfonic acid monohydrate / 0.33 h / Heating

3: 25 g / triethylamine / tetrahydrofuran / 0.5 h / Ambient temperature

4: 0.5 M H₂SO₄ / acetone / 0.08 h / Heating

With hydrogenchloride; sulfuric acid; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)81431-9