4-(benzoyloxy)-3-iodobenzaldehyde

Base Information

Chemical Name:4-(benzoyloxy)-3-iodobenzaldehyde
CAS No.:147672-98-8
Molecular Formula:C₁₄H₉IO₃
Molecular Weight:352.128
Hs Code.:

Synonyms:4-(benzoyloxy)-3-iodobenzaldehyde

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Chemical Property of 4-(benzoyloxy)-3-iodobenzaldehyde

Chemical Property:

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Technology Process of 4-(benzoyloxy)-3-iodobenzaldehyde

There total 2 articles about 4-(benzoyloxy)-3-iodobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 60032-63-5
4-hydroxy-3-iodo-benzaldehyde

: 98-88-4
benzoyl chloride

: 147672-98-8
4-(benzoyloxy)-3-iodobenzaldehyde

Guidance literature:: With triethylamine; In diethyl ether; for 0.5h; Ambient temperature;
DOI:10.1002/hlca.19930760126

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 147672-98-8
4-(benzoyloxy)-3-iodobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / I₂, KI, aq. Me₂NH / 3 h / Ambient temperature

2: 83 percent / NEt₃ / diethyl ether / 0.5 h / Ambient temperature

With iodine; dimethyl amine; triethylamine; potassium iodide; In diethyl ether;
DOI:10.1002/hlca.19930760126

Reference yield:

: 147672-98-8
4-(benzoyloxy)-3-iodobenzaldehyde

: 121007-19-0
4-hydroxy-3-(3′-methylbut-3′-en-1′-ynyl)-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1) CuI, aq. NH₄OH, NH₂OH*HCl / 1) EtOH, 15 min, 2) DMF, 110 to 120 deg C, 3 h

2: 62 percent / 3percent aq. NaOH / ethanol / 2 h

3: 79 percent / NaClO₂, sulfamic acid / H₂O; dioxane / 1 h / Ambient temperature

With ammonium hydroxide; sodium hydroxide; sodium chlorite; copper(l) iodide; aminosulfonic acid; hydroxylamine hydrochloride; In 1,4-dioxane; ethanol; water;
DOI:10.1002/hlca.19930760126