methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

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Chemical Name:methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate
CAS No.:118607-94-6
Molecular Formula:C₂₀H₃₀O₇
Molecular Weight:382.454
Hs Code.:

Synonyms:methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

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Technology Process of methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

There total 9 articles about methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 118649-30-2
methyl (E)-2,4-di(methoxymethoxy)-6-methyl-3<(6-O-tert-butyldimethylsilyl-3-methyl)-2-hexenyl>-benzoate

: 118607-94-6
methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h;
DOI:10.1016/S0040-4020(01)85090-0

Reference yield:

: 1071-73-4
5-Hydroxy-2-pentanone

: 118607-94-6
methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / imidazole / dimethylformamide / 24 h / 70 °C

2: 17.25 g / NaH / tetrahydrofuran; hexane; diethyl ether / 40 h / Ambient temperature

3: 96 percent / DIBAL / CH₂Cl₂ / -78 deg C, 1 h, then 0 deg C

4: CBr₄, Ph₃P / CH₂Cl₂ / 1 h / -78 °C

5: 3.10 g / toluene / 12 h / Heating

6: 66 percent / NaH / CH₂Cl₂ / 1 h / Ambient temperature

7: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h

With 1H-imidazole; carbon tetrabromide; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4020(01)85090-0

Reference yield:

: 3187-58-4
methyl orsellinate

: 118607-94-6
methyl (E)-3,4-di(methoxymethoxy)-6-methyl-3<(3-methyl-6-ol)-2-hexenyl>-benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / KOH / ethanol / Ambient temperature

2: 3.10 g / toluene / 12 h / Heating

3: 66 percent / NaH / CH₂Cl₂ / 1 h / Ambient temperature

4: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h

With potassium hydroxide; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)85090-0