methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

Base Information

Chemical Name:methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate
CAS No.:1262841-28-0
Molecular Formula:C₁₄H₁₆F₃NO₅
Molecular Weight:335.28
Hs Code.:

Synonyms:methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

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Chemical Property of methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

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Technology Process of methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

There total 1 articles about methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67-56-1
methanol

: 58137-35-2
methyl 2-(trifluoroacetamido)acrylate

: 459-64-3
4-methoxybenzenediazonium tetrafluoroborate

: 1262841-28-0
methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; palladium diacetate; at 65 ℃;
DOI:10.1016/j.tetlet.2010.10.132

Reference yield: 36.0%

: 1262841-28-0
methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

: 1262841-35-9
methyl 23-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

: 128070-29-1
(E)-3-(4-Methoxy-phenyl)-2-(2,2,2-trifluoro-acetylamino)-acrylic acid methyl ester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; phenylsilane; In 1,2-dichloro-ethane; at 0 - 83 ℃; for 17h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.10.132

Reference yield: 32.0%

: 1262841-28-0
methyl 2-methoxy-3-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

: 1262841-35-9
methyl 23-(4-methoxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 0 - 83 ℃; for 120h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.10.132