C₂₃H₂₉NO

Base Information

• Chemical Name: C₂₃H₂₉NO
• CAS No.: 952062-44-1
• Molecular Formula: C₂₃H₂₉NO
• Molecular Weight: 335.489

Synonyms:C₂₃H₂₉NO

Chemical Property of C₂₃H₂₉NO

Chemical Property:

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Technology Process of C₂₃H₂₉NO

There total 3 articles about C₂₃H₂₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-5-benzyloxy-2-pentenyl methyl carbonate → C23H29NO (952062-44-1)

Guidance literature:

Multi-step reaction with 2 steps

1: chiral binaphthyl-based reagent; [Ir(COD)Cl]2; n-propylamine / tetrahydrofuran / 10 h / 20 °C

2: sodium hydrogen carbonate; n-Bu₄NI / acetonitrile / 12 h / Heating

With propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; chiral binaphthyl-based reagent; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo070998h

Reference yield:

benzylamine (100-46-9) → C23H29NO (952062-44-1)

Guidance literature:

Multi-step reaction with 2 steps

1: chiral binaphthyl-based reagent; [Ir(COD)Cl]2; n-propylamine / tetrahydrofuran / 10 h / 20 °C

2: sodium hydrogen carbonate; n-Bu₄NI / acetonitrile / 12 h / Heating

With propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; chiral binaphthyl-based reagent; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo070998h

Reference yield:

1-bromo-4-butene (5162-44-7) + (R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine (952062-42-9) → C23H29NO (952062-44-1)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; In acetonitrile; for 12h; Heating;

DOI:10.1021/jo070998h

upstream raw materials:

1-bromo-4-butene

(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

benzylamine

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