ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid

Base Information

• Chemical Name: ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid
• CAS No.: 128462-69-1
• Molecular Formula: C₁₂H₁₄N₂O₄
• Molecular Weight: 250.254
• Mol file: 128462-69-1.mol

Synonyms:ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid

Chemical Property of ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid

There total 1 articles about ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

ethyl 2-hydrazino-2-oxoacetate (35196-48-6) + ortho-anisaldehyde (135-02-4) → ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid (128462-69-1)

Guidance literature:

In water; at 25 ℃; for 7h; Green chemistry;

DOI:10.1016/j.tetlet.2018.04.047

Reference yield: 63.0%

4-(3-Aminopropyl)morpholine (123-00-2) + ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid (128462-69-1) → C17H24N4O4

Guidance literature:

In ethanol; at 85 ℃;

DOI:10.1016/j.ejmech.2019.04.006

Reference yield: 63.0%

n-butyl magnesium bromide (693-03-8) + ethyl ester of the o-methoxybenzylidenehydrazide of oxalic acid (128462-69-1) → 2-Butyl-2-hydroxy-hexanoic acid [1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide (128462-79-3)

Guidance literature:

at 0 ℃; for 0.666667h;

upstream raw materials:

ethyl 2-hydrazino-2-oxoacetate

ortho-anisaldehyde

Downstream raw materials:

2-Butyl-2-hydroxy-hexanoic acid [1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

2-Benzyl-2-hydroxy-3-phenyl-propionic acid [1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Hydroxy-diphenyl-acetic acid [1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Bis-(4-chloro-phenyl)-hydroxy-acetic acid [1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide