16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

Base Information

Chemical Name:16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol
CAS No.:929683-38-5
Molecular Formula:C₃₃H₄₄N₂O₄
Molecular Weight:532.723
Hs Code.:

Synonyms:16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

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Chemical Property of 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

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Technology Process of 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

There total 3 articles about 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.68%

: 67-56-1
methanol

: 929683-36-3
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxy-benzylidene]-17-oxo-5-androsten-3β-ol

: 929683-38-5
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

Guidance literature:: With sodium tetrahydroborate; at 20 ℃; for 8h;

Reference yield:

: 151719-92-5
3-methoxy-4-(3-chloropropoxy) benzaldehyde

: 929683-38-5
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 2 h / 20 °C

2: 5 h / 110 - 120 °C

3: sodium tetrahydroborate / 8 h / 20 °C

With sodium tetrahydroborate; sodium hydroxide; In methanol;

Reference yield:

: 53-43-0
dehydroepiandrosterone

: 929683-38-5
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-5-androstene-3β,17β-diol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 2 h / 20 °C

2: 5 h / 110 - 120 °C

3: sodium tetrahydroborate / 8 h / 20 °C

With sodium tetrahydroborate; sodium hydroxide; In methanol;