Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

Base Information

Chemical Name:Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester
CAS No.:106470-33-1
Molecular Formula:C₂₉H₄₀O₃S₂
Molecular Weight:500.767
Hs Code.:

Synonyms:Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

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Chemical Property of Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

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Technology Process of Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

There total 7 articles about Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 35733-58-5
tetra(n-butyl)ammonium formate

: 106470-32-0
(Z)-(1RS,3SR,4SR,5SR)-4-<7-<(methanesulfonyl)oxy>-2-heptenyl>-5-<1-(4-methoxyphenyl)non-2-ynylthio>-2-thiabicyclo<3.1.0>hexane

: 106470-33-1
Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 2h;
DOI:10.1021/jo00381a027

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 106470-33-1
Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CHCl₃ / 1.5 h / 22 °C

2: 100 percent / triethylamine / CH₂Cl₂ / 0.67 h / 0 °C

4: 100 percent / dimethylformamide / 2 h / 60 °C

With triethylamine; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00381a027

Reference yield:

: 106470-29-5
(Z)-(1RS,2RS,3RS,4SR)-2-hydroxy-3-(7-hydroxy-2-heptenyl)cyclopentane 1,4-dithiol

: 106470-33-1
Formic acid (Z)-7-{(1R,2R,3R,5S)-3-[1-(4-methoxy-phenyl)-non-2-ynylsulfanyl]-6-thia-bicyclo[3.1.0]hex-2-yl}-hept-5-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CHCl₃ / 1.5 h / 22 °C

2: 100 percent / triethylamine / CH₂Cl₂ / 0.67 h / 0 °C

4: 100 percent / dimethylformamide / 2 h / 60 °C

With triethylamine; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00381a027