C₂₈H₂₉N₅O₅

Base Information

Chemical Name:C₂₈H₂₉N₅O₅
CAS No.:1622205-37-1
Molecular Formula:C₂₈H₂₉N₅O₅
Molecular Weight:515.569
Hs Code.:

C<sub>28</sub>H<sub>29</sub>N<sub>5</sub>O<sub>5</sub>

Synonyms:C₂₈H₂₉N₅O₅

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Chemical Property of C₂₈H₂₉N₅O₅

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Technology Process of C₂₈H₂₉N₅O₅

There total 14 articles about C₂₈H₂₉N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1622205-36-0
C₃₃H₃₇N₅O₇

: 1622205-37-1
C₂₈H₂₉N₅O₅

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 1.25h;

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 1622205-37-1
C₂₈H₂₉N₅O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetic acid; ammonium acetate / 2.33 h / 130 °C / Inert atmosphere

2.1: acetic acid; nitric acid / 3 h / 25 - 40 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol; water / 3 h

4.1: potassium tert-butylate / dimethyl sulfoxide / 12.5 h / 160 °C / Inert atmosphere

5.1: methanol; sodium methylate / 5.5 h / 20 - 70 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C / Inert atmosphere

6.2: 3 h / 0 - 20 °C

7.1: 1,2,3-Benzotriazole; thionyl chloride / dichloromethane / 0.42 h / 20 °C / Inert atmosphere

7.2: 1.5 h / 0 - 20 °C

8.1: trifluoroacetic acid / dichloromethane / 1.25 h / 0 - 20 °C

With methanol; 1,2,3-Benzotriazole; thionyl chloride; palladium 10% on activated carbon; potassium tert-butylate; ammonium acetate; hydrogen; nitric acid; sodium methylate; sodium hydride; acetic acid; trifluoroacetic acid; In methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 1622205-37-1
C₂₈H₂₉N₅O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C

2.1: ethanol; sodium hydroxide / 7 h / 50 °C

3.1: 1,2,3-Benzotriazole; thionyl chloride / dichloromethane / 0.42 h / 20 °C / Inert atmosphere

3.2: 1.5 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 1.25 h / 0 - 20 °C

With 1,2,3-Benzotriazole; thionyl chloride; ethanol; di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane;