C₃₃H₄₃FN₄O₅

Base Information

Chemical Name:C₃₃H₄₃FN₄O₅
CAS No.:1624627-61-7
Molecular Formula:C₃₃H₄₃FN₄O₅
Molecular Weight:594.727
Hs Code.:

C<sub>33</sub>H<sub>43</sub>FN<sub>4</sub>O<sub>5</sub>

Synonyms:C₃₃H₄₃FN₄O₅

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Chemical Property of C₃₃H₄₃FN₄O₅

Chemical Property:

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Technology Process of C₃₃H₄₃FN₄O₅

There total 8 articles about C₃₃H₄₃FN₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1624627-59-3
1,3,2’,6’-tetraazido-5,6,3’-tri-O-benzyl-4’-deoxy-4’-fluoro-4’-epineamine

: 1624627-61-7
C₃₃H₄₃FN₄O₅

Guidance literature:: With water; sodium hydroxide; trimethylphosphane; In tetrahydrofuran; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c4md00072b

Reference yield:

: 1624627-55-9
1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

: 1624627-61-7
C₃₃H₄₃FN₄O₅

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; water / tetrahydrofuran / 60 °C / Inert atmosphere

2: pyridine / dichloromethane / 22 - 26 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

4: diethylamino-sulfur trifluoride / dichloromethane / 22 - 26 °C / Inert atmosphere

5: trimethylphosphane; sodium hydroxide; water / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

With pyridine; sodium azide; diethylamino-sulfur trifluoride; water; acetic acid; sodium hydroxide; trimethylphosphane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 5: |Staudinger Azide Reduction;
DOI:10.1039/c4md00072b

Reference yield:

: 1604038-74-5
1,3,2’-triazido-4’,6’-O-benzylideneparomamine

: 1624627-61-7
C₃₃H₄₃FN₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 26 °C

2.1: acetic acid; water / tetrahydrofuran / 60 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 22 - 26 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

5.1: diethylamino-sulfur trifluoride / dichloromethane / 22 - 26 °C / Inert atmosphere

6.1: trimethylphosphane; sodium hydroxide; water / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

With pyridine; sodium azide; diethylamino-sulfur trifluoride; water; sodium hydride; acetic acid; sodium hydroxide; trimethylphosphane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil; 6.1: |Staudinger Azide Reduction;
DOI:10.1039/c4md00072b