1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

Base Information

Chemical Name:1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine
CAS No.:1624627-55-9
Molecular Formula:C₄₀H₄₁N₉O₇
Molecular Weight:759.822
Hs Code.:

Synonyms:1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

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Chemical Property of 1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

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Technology Process of 1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

There total 4 articles about 1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1604038-74-5
1,3,2’-triazido-4’,6’-O-benzylideneparomamine

: 100-39-0
benzyl bromide

: 1624627-55-9
1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

Guidance literature:: 1,3,2’-triazido-4’,6’-O-benzylideneparomamine; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1h; Inert atmosphere;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 0 - 26 ℃;
DOI:10.1039/c4md00072b

Reference yield:

: 289505-10-8
(2R,3S,4R,5R,6S)-5-azido-6-(((1R,2R,3S,4R,6S)-4, 6-diazido-2,3-dihydroxycyclohexyl)oxy)-2-(hydroxymethyl)tetrahydro-2H-pyran-3,4-diol

: 1624627-55-9
1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1S)-10-camphorsulfonic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere

2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.2: 0 - 26 °C

With (1S)-10-camphorsulfonic acid; sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane; mineral oil;
DOI:10.1039/c4md00072b

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 1624627-55-9
1,3,2’-triazido-5,6,3’-tri-O-benzyl-4’,6’-O-benzylidene paromamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1S)-10-camphorsulfonic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere

2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.2: 0 - 26 °C

With (1S)-10-camphorsulfonic acid; sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane; mineral oil;
DOI:10.1039/c4md00072b