4-carbamoyldiphenyl sulfide

Base Information

• Chemical Name: 4-carbamoyldiphenyl sulfide
• CAS No.: 29921-16-2
• Molecular Formula: C₁₃H₁₁NOS
• Molecular Weight: 229.302
• Mol file: 29921-16-2.mol

Synonyms:4-carbamoyldiphenyl sulfide

Chemical Property of 4-carbamoyldiphenyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-carbamoyldiphenyl sulfide

There total 3 articles about 4-carbamoyldiphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-Cyanochlorobenzene (623-03-0) + sodium thiophenolate (930-69-8) → 4-carbamoyldiphenyl sulfide (29921-16-2)

Guidance literature:

With water; o-phenylene-bis-nickel(II) bromide; In ethylene glycol; at 200 ℃; for 24h;

DOI:10.1055/s-1981-29636

Reference yield:

thiophenol (108-98-5) → 4-carbamoyldiphenyl sulfide (29921-16-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Na / diethyl ether / 24 h

2: 80 percent / H₂O / o-phenylene-bis-nickel(II) bromide / ethane-1,2-diol / 24 h / 200 °C

With water; sodium; o-phenylene-bis-nickel(II) bromide; In diethyl ether; ethylene glycol;

DOI:10.1055/s-1981-29636

Reference yield:

→ 4-carbamoyldiphenyl sulfide (29921-16-2)

Guidance literature:

entspr. Saeurechlorid, NH4OH;

upstream raw materials:

4-Cyanochlorobenzene

sodium thiophenolate

thiophenol