(η(1)-phenyl)trioxorhenium

Base Information

Chemical Name:(η(1)-phenyl)trioxorhenium
CAS No.:131457-04-0
Molecular Formula:C₆H₅O₃Re
Molecular Weight:311.311
Hs Code.:

Synonyms:(η(1)-phenyl)trioxorhenium

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Chemical Property of (η(1)-phenyl)trioxorhenium

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Technology Process of (η(1)-phenyl)trioxorhenium

There total 2 articles about (η(1)-phenyl)trioxorhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138693-72-8
phenyltrioxo(tetrahydrofuran)rhenium(VII)

: 131457-04-0
(η(1)-phenyl)trioxorhenium

Guidance literature:: In neat (no solvent); under N2, removal of THF under vacuum (2 h); elem. anal.;

Reference yield:

: 1078-58-6
diphenylzinc

: rhenium(VII) oxide

: 131457-04-0
(η(1)-phenyl)trioxorhenium

Guidance literature:: In tetrahydrofuran; byproducts: {Zn(ReO4)2(C4H8O)2}; addn. of Zn-compd. to soln. of Re2O7 at dry-ice temp., warmed up to -5°C; extd. (cold pentane), volume reduced (vac., -30°C), crystn. on dry-ice, dried (high-vac., -30°C); GC-MS;