3-chlorophenyl N,N-diethylcarbamate

Base Information

Chemical Name:3-chlorophenyl N,N-diethylcarbamate
CAS No.:159390-33-7
Molecular Formula:C₁₁H₁₄ClNO₂
Molecular Weight:227.691
Hs Code.:

Synonyms:3-chlorophenyl N,N-diethylcarbamate

Suppliers and Price of 3-chlorophenyl N,N-diethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 3-chlorophenyl N,N-diethylcarbamate

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-chlorophenyl N,N-diethylcarbamate

There total 1 articles about 3-chlorophenyl N,N-diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-43-0
3-monochlorophenol

: 88-10-8
N,N-diethylcarbamyl chloride

: 159390-33-7
3-chlorophenyl N,N-diethylcarbamate

Guidance literature:: With potassium carbonate; In acetonitrile; at 70 ℃; for 13.5h;
DOI:10.1016/j.ejmech.2010.07.044

Reference yield: 89.0%

: 75-77-4
chloro-trimethyl-silane

: 159390-33-7
3-chlorophenyl N,N-diethylcarbamate

: O-(2-trimethylsilyl-3-chloro)phenyl N,N-diethylcarbamate

Guidance literature:: 3-chlorophenyl N,N-diethylcarbamate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; for 8h; Inert atmosphere;
DOI:10.1002/ejoc.201701143