6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone

Base Information

• Chemical Name: 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone
• CAS No.: 111794-36-6
• Molecular Formula: C₂₀H₂₂N₄O₂
• Molecular Weight: 350.42

Synonyms:6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone

Chemical Property of 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone

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Technology Process of 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone

There total 2 articles about 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

6-<4-(3-bromopropionamido)phenyl>-4,5-dihydro-3(2H)-pyridazinone (111794-33-3) + benzylamine (100-46-9) → 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone (111794-36-6)

Guidance literature:

In propan-1-ol; for 16h; Heating;

DOI:10.1021/jm00397a013

Reference yield:

6-(4-aminophenyl)-4,5-dihydro-3(2H)-pyridazinone (21282-90-6) → 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone (111794-36-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / toluene / 16 h / Heating

2: 42 percent / propan-1-ol / 16 h / Heating

In propan-1-ol; toluene;

DOI:10.1021/jm00397a013

Reference yield: 75.0%

o-Cresyl glycidyl ether (2210-79-9) + 6-<4-<3-(benzylamino)propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone (111794-36-6) → 6-<4-<3-amino>propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone (111794-45-7)

Guidance literature:

In propan-1-ol; for 16h; Heating;

DOI:10.1021/jm00397a013

upstream raw materials:

6-<4-(3-bromopropionamido)phenyl>-4,5-dihydro-3(2H)-pyridazinone

benzylamine

6-(4-aminophenyl)-4,5-dihydro-3(2H)-pyridazinone

Downstream raw materials:

6-<4-<3-amino>propionamido>phenyl>-4,5-dihydro-3(2H)-pyridazinone

3-{Benzyl-[3-(2-cyano-phenoxy)-2-hydroxy-propyl]-amino}-N-[4-(6-oxo-1,4,5,6-tetrahydro-pyridazin-3-yl)-phenyl]-propionamide

3-{Benzyl-[2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-amino}-N-[4-(6-oxo-1,4,5,6-tetrahydro-pyridazin-3-yl)-phenyl]-propionamide

6-[4-(3-{[2-hydroxy-3-(2-methylphenoxy)propyl]amino}propionamido)phenyl]-4,5-dihydro-3(2H)-pyridazinone

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