DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

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Chemical Name:DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>
CAS No.:112424-11-0
Molecular Formula:C₂₇H₂₀F₆O₆S₆
Molecular Weight:746.839
Hs Code.:

DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

Synonyms:DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

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Chemical Property of DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

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Technology Process of DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

There total 6 articles about DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 112424-09-6
DL-(1α,2α,3α,4α,5β,6β)-1,2:3,4-Bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

: 7143-01-3
Methanesulfonic anhydride

: 112424-11-0
DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

Guidance literature:: With triethylamine; In dichloromethane; 1.) 30 min, 0 deg C; 2.) 2 h, RT;

Reference yield:

: 39078-11-0
cis-trisoxirane

: 112424-11-0
DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NaOCH₃ / methanol / 1 h / Heating

2: 98 percent / NEt₃ / CH₂Cl₂ / 8 h / Ambient temperature

3: 65 percent / KOH / tetrahydrofuran / 5 h / 50 °C

4: 90 percent / NEt₃ / CH₂Cl₂ / 1.) 30 min, 0 deg C; 2.) 2 h, RT

With potassium hydroxide; sodium methylate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 39234-86-1
3,5-bis(trifluoromethyl)benzenesulfonyl chloride

: 112424-11-0
DL-(1α,2α,3α,4α,5β,6β)-6-O-(Methylsulfonyl)-1,2:3,4-bis-S-(1,2-phenylen)-1,2,3,4-tetrathio-1,2,3,4,5,6-cyclohexanhexol-5-<3,5-bis(trifluormethyl)benzolsulfonat>

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NEt₃ / CH₂Cl₂ / 8 h / Ambient temperature

2: 65 percent / KOH / tetrahydrofuran / 5 h / 50 °C

3: 90 percent / NEt₃ / CH₂Cl₂ / 1.) 30 min, 0 deg C; 2.) 2 h, RT

With potassium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane;