2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on

Base Information

Chemical Name:2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on
CAS No.:52751-37-8
Molecular Formula:C₆F₃N₃O₃
Molecular Weight:219.08
Hs Code.:

Synonyms:2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on

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Chemical Property of 2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on

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Technology Process of 2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on

There total 2 articles about 2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6157-98-8
2,3,4,5-tetrafluoro-6-nitroaniline

: 52751-37-8
2-Azo-3-nitrotrifluor-3,5-cyclohexadien-1-on

Guidance literature:: With sulfuric acid; nitric acid; sodium nitrite; oxidation with concd. HNO3 at 65-75°C 1 h, then diazotation with NaNO2 in 70% H2SO4 at -15 to -12°C 0.25 h, then stirring at 10-20°C 2 h;
DOI:10.1016/S0022-1139(00)82509-9