ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol

Base Information

Chemical Name:ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol
CAS No.:134734-27-3
Molecular Formula:C₂₂H₂₈O₈S₂
Molecular Weight:484.592
Hs Code.:

Synonyms:ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol

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Chemical Property of ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol

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Technology Process of ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol

There total 7 articles about ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134936-48-4
3-Ethyl-2,3-dihydro-furan-3-carboxylic acid methyl ester

: 134734-27-3
C₂₂H₂₈O₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1: m-chloroperbenzoic acid / 1 h / 0 °C

2: pyridine / Ambient temperature

3: LiAlH₄ / diethyl ether / 3 h / Heating

4: pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether;
DOI:10.1002/jhet.5570280315

Reference yield:

: 134936-48-4
3-Ethyl-2,3-dihydro-furan-3-carboxylic acid methyl ester

: 134734-27-3
ditosylate of threo-4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: m-chloroperbenzoic acid / 1 h / 0 °C

2: pyridine / Ambient temperature

3: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

4: 61 percent / pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether;
DOI:10.1002/jhet.5570280315

Reference yield:

: methyl 4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-carboxylate

: 134734-27-3
C₂₂H₂₈O₈S₂

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / Ambient temperature

2: LiAlH₄ / diethyl ether / 3 h / Heating

3: pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1002/jhet.5570280315