4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

Base Information

Chemical Name:4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide
CAS No.:716317-12-3
Molecular Formula:C₂₉H₄₀N₂O₃SSi
Molecular Weight:524.8
Hs Code.:

Synonyms:4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

Suppliers and Price of 4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

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Technology Process of 4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

There total 3 articles about 4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 716317-11-2
4'-(2-hydroxybenzylamino)biphenyl-2-N-tert-butylsulfonamide

: 716317-12-3
4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.3987/com-04-10022

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 716317-12-3
4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 0.5 h / Heating

1.2: 63 percent / sodium borohydride / ethanol / 16 h / 20 °C

2.1: 88 percent / diisopropylethylamine / CH₂Cl₂ / 20 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.3987/com-04-10022

Reference yield:

: 193006-34-7
4-(2'-tert-butylaminosulfonylphenyl)aniline

: 716317-12-3
4'-[2-(tert-butyldimethylsilyloxy)benzylamino]biphenyl-2-N-tert-butylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 0.5 h / Heating

1.2: 63 percent / sodium borohydride / ethanol / 16 h / 20 °C

2.1: 88 percent / diisopropylethylamine / CH₂Cl₂ / 20 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.3987/com-04-10022