sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

Base Information

Chemical Name:sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate
CAS No.:866146-53-4
Molecular Formula:C₁₀H₁₀Cl₂O₆P*Na
Molecular Weight:351.055
Hs Code.:

Synonyms:sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

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Chemical Property of sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

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Technology Process of sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

There total 5 articles about sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (2,4-dichloro-phenoxy)-acetic acid 1-phosphono-ethyl ester

: 866146-53-4
sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 2h;
DOI:10.1080/10426507.2012.717147

Reference yield:

: C₁₆H₂₇Cl₂O₆PSi₂

: 866146-53-4
sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 30 °C

2: sodium hydroxide / methanol / 2 h / 20 °C

With methanol; sodium hydroxide; In methanol;
DOI:10.1080/10426507.2012.717147

Reference yield:

: 774-74-3
2-(2,4-dichlorophenoxy)acetyl chloride

: 866146-53-4
sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}ethyl)phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 4 h / 5 °C

2: sodium iodide / acetonitrile / 2 h / 30 °C / Inert atmosphere; Darkness

3: methanol / 30 °C

4: sodium hydroxide / methanol / 2 h / 20 °C

With pyridine; methanol; sodium iodide; sodium hydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1080/10426507.2012.717147