ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride

Base Information

• Chemical Name: ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride
• CAS No.: 96229-31-1
• Molecular Formula: C₁₂H₁₈N₂O₃S*ClH
• Molecular Weight: 306.813

Synonyms:ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride

Chemical Property of ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride

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Technology Process of ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride

There total 4 articles about ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethanol (64-17-5) + N-(β-cyanoethyl)-p-toluenesulfonamide (2619-22-9) → ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride (96229-31-1)

Guidance literature:

With hydrogenchloride; In diethyl ether; at 5 ℃; for 18h;

DOI:10.1039/b404962d

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride (96229-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / Et₃N / CH₂Cl₂ / 0.17 h / 0 °C

2: 100 percent / HCl / diethyl ether / 18 h / 5 °C

With hydrogenchloride; triethylamine; In diethyl ether; dichloromethane;

DOI:10.1039/b404962d

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride (96229-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / NaOH / H₂O; ethyl acetate / pH 10

2: 80 percent / HCl / diethyl ether / 0 - 4 °C

With hydrogenchloride; sodium hydroxide; In diethyl ether; water; ethyl acetate; 2: Pinner reaction;

DOI:10.1016/j.bmc.2005.12.043

upstream raw materials:

ethanol

N-(β-cyanoethyl)-p-toluenesulfonamide

p-toluenesulfonyl chloride

Downstream raw materials:

N-{2-[5-(4-chloro-phenyl)-[1,3,4]oxadiazol-2-yl]-ethyl}-toluene-4-sulfonamide

N-{2-[5-(4-nitro-phenyl)-[1,3,4]oxadiazol-2-yl]-ethyl}-toluene-4-sulfonamide

N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

N-[2-(5-phenyl-[1,3,4]oxadiazol-2-yl)-ethyl]-toluene-4-sulfonamide

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