5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester

Base Information

• Chemical Name: 5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester
• CAS No.: 268539-18-0
• Molecular Formula: C₁₇H₁₃N₅O₈
• Molecular Weight: 415.319
• Mol file: 268539-18-0.mol

Synonyms:5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester

Chemical Property of 5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester

Chemical Property:

Purity/Quality:

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Technology Process of 5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester

There total 1 articles about 5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + 5-azidomethylbenzene-1,3-dicarboxylic acid (252210-02-9) → 5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester (268539-18-0)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 25 ℃; for 18h;

DOI:10.1016/S0957-4166(99)00589-3

Reference yield: 63.0%

5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester (268539-18-0) + C53H79N3O28 → 5-azidomethyl-N,N'-bis-1-phenylmethyl-3,5-dicarboxamide>benzene-1,3-dicarboxamide

Guidance literature:

With triethylamine; In tetrahydrofuran; at 25 ℃; for 0.8h;

DOI:10.1016/S0957-4166(99)00589-3

Reference yield: 47.0%

5-azidomethylbenzene-1,3-dicarboxylate di-N-hydroxysuccinimide ester (268539-18-0) + C49H67N7O26 → 5-azidomethyl-N,N'-bis-1-phenylmethyl-3,5-dicarboxamide>benzene-1,3-dicarboxamide

Guidance literature:

With triethylamine; In tetrahydrofuran; at 25 ℃; for 168h;

DOI:10.1016/S0957-4166(99)00589-3

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

5-azidomethylbenzene-1,3-dicarboxylic acid