ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

Base Information

Chemical Name:ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate
CAS No.:857463-56-0
Molecular Formula:C₂₉H₄₂O₃
Molecular Weight:438.651
Hs Code.:

Synonyms:ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

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Technology Process of ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

There total 5 articles about ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 857463-55-9
(E,E,E)-14-benzyloxy-4,8,12-trimethyl-4,8,12-hexadecatrienal

: 21382-82-1
(carbethoxyethylidene)triphenylphosphorane

: 857463-56-0
ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

Guidance literature:: In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo0502091

Reference yield:

: (E,E,E)-16-benzyloxy-2,3-epoxy-2,6,10,14-tetramethyl-6,10,14-hexadecatriene

: 857463-56-0
ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / HClO₄ / tetrahydrofuran; H₂O / 0.83 h / 20 °C

2: 96 percent / NaIO₄ / tetrahydrofuran; H₂O / 17 h / 20 °C

3: 98 percent / CH₂Cl₂ / 0 - 20 °C

With sodium periodate; perchloric acid; In tetrahydrofuran; dichloromethane; water; 3: Wittig reaction;
DOI:10.1021/jo0502091

Reference yield:

: (E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-6,10,14-hexadecatrien-2,3-diol

: 857463-56-0
ethyl (E,E,E,E)-16-benzyloxy-2,6,10,14-tetramethyl-2,6,10,14-hexadecatetraenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaIO₄ / tetrahydrofuran; H₂O / 17 h / 20 °C

2: 98 percent / CH₂Cl₂ / 0 - 20 °C

With sodium periodate; In tetrahydrofuran; dichloromethane; water; 2: Wittig reaction;
DOI:10.1021/jo0502091