N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Base Information

Chemical Name:N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide
CAS No.:1400700-98-2
Molecular Formula:C₂₄H₂₂N₆O₄
Molecular Weight:458.476
Hs Code.:

Synonyms:N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

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Chemical Property of N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

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Technology Process of N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

There total 6 articles about N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1400700-92-6
C₁₆H₁₆N₆O₃

: 123-11-5
4-methoxy-benzaldehyde

: 1400700-98-2
N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Guidance literature:: With acetic acid; In ethanol; for 5h; Reflux;
DOI:10.1016/j.ejmech.2012.06.048

Reference yield:

: 177662-77-0
C₁₄H₁₄N₄O

: 1400700-98-2
N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 3 h / 20 °C

2: 2 h / Reflux

3: hydrazine hydrate / ethanol / 5 h / 20 °C

4: acetic acid / ethanol / 5 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol; benzene;
DOI:10.1016/j.ejmech.2012.06.048

Reference yield:

: C₁₆H₁₃ClN₄O₃

: 1400700-98-2
N'-(4-methoxybenzylidene)-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 2 h / Reflux

2: hydrazine hydrate / ethanol / 5 h / 20 °C

3: acetic acid / ethanol / 5 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/j.ejmech.2012.06.048