(E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

Base Information

Chemical Name:(E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide
CAS No.:1562381-49-0
Molecular Formula:C₁₈H₁₆ClNO₂S
Molecular Weight:345.85
Hs Code.:

Synonyms:(E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

Suppliers and Price of (E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

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Technology Process of (E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

There total 2 articles about (E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₆BrCl

: 640-61-9
N-methyl-p-toluenesulfonylamide

: 1562381-49-0
(E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; In toluene; at 80 ℃; Inert atmosphere; Sealed tube;
DOI:10.1021/ja412634w

Reference yield:

: 53081-61-1
(E)-1-(but-1-en-3-yn-1-yl)-4-chlorobenzene

: 1562381-49-0
(E)-N-(4-(4-chlorophenyl)but-3-en-1-yn-1-yl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; silver nitrate / acetone / 1 h / 20 °C / Inert atmosphere

2: 1,10-Phenanthroline; potassium carbonate; copper(ll) sulfate pentahydrate / toluene / 80 °C / Inert atmosphere; Sealed tube

With N-Bromosuccinimide; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; silver nitrate; In acetone; toluene;
DOI:10.1021/ja412634w